ABOUT THE COURSE INTENDED AUDIENCE Undergraduate
students of Metallurgical and Materials, Physics, Chemistry and biological
sciences
It is the first course at the under graduate level on
microstructural characterization of materials. This course will cover the
basic principles and techniques of X-ray diffraction, optical, scanning electron and transmission
electron microscopy along with demonstrations of the instrument details and imaging
experiments through videos. This
course also deals with the sample preparation techniques for the
microstructural analysis with practical examples through videos.
PRE-REQUISITES
N/A
INDUSTRY SUPPORT – LIST OF COMPANIES/INDUSTRY THAT WILL RECOGNIZE/VALUE THIS ONLINE COURSE
All the Metallurgical and automotive industries will
be interested in this course
COURSE INSTRUCTOR
Week 1
1. Fundamentals of optics
2. Optical microscope and its instrumental details
Week 2
3. Variants in the optical microscopes and image formation
4. Phase contrast, Polarised light, Differential interference contrast, Fluorescence microscopy
Week 3
5. Sample preparation and applications of optical microscopes
Week 4
6. Introduction to Scanning electron microscopy (SEM)
Week 5
7. Instrumental details and image formation of SEM
Week 6
8. Various imaging techniques and spectroscopy
9. Sample preparation and applications of SEM
Week 7
10. Fundamentals of X-ray scattering
11. Bragg’s law derivation and the factors affecting the intensity
Week 8
12. Crystallite size, effect of strain on the intensity
13. Profile fit, indexing, peak broadening
Week 9
14. Quantitative analysis, residual stress analysis
15. Instrumentation details and demo experiments of XRD
Week 10
16. Introduction to transmission electron microscopy (TEM)
Week 11
18. Various imaging techniques and spectroscopy
Week 12
20. Instrumentation details and demo experiments of TEM
LIST OF REFERENCE MATERIALS / BOOKS
1) ‘Fundamentals of light microscopy and electronic imaging’ Douglas B. Murphy, 2001, Wiley-Liss, Inc. USA
2) ‘Encyclopedia of Materials Characterization, Surfaces, Interfaces, Thin Films,’ Editors C. Richard Brundle, Charles A. Evans, Jr., Shaun Wilson, Butterworth-Heinemann, Boston, USA
3) ‘Elements of X-ray diffraction’ B.D. Cullity and S.R. Stock, 2001, Prentice Hall, Inc. USA
4) ‘Transmission electron microscopy” D.B. Williams and C. Barry Carter, 4 volumes, Springer, 1996. USA